1-氯-6H-十二氟己烷合成路线 （共 44 条）
反应条件
1: (FSO2O)2 2: ClOSO2F, HSO3F, SbF5 3: KF / bis-(2-methoxy-ethyl) ether View Scheme
参考文献
Rapkin, A. I.; Zabolot-skikh, V. F.; Kochanov, A. S.; Tiunov, A. V.; Zhirnov, O. M.
Russian Journal of Applied Chemistry, 1995 , vol. 68, # 1part2 p. 133 - 134
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1995 , vol. 68, # 1 p. 151 - 152
反应条件
hydrazine hydrate; zinc in N,N-dimethyl-formamide T=70°C; 2 h;
参考文献
Wu, Fang-Hong; Huang, Bing-Nan; Huang, Wei-Yuan
Journal of Fluorine Chemistry, 1995 , vol. 73, # 2 p. 159 - 160
反应条件
chlorine; nitrogen(IV) oxide T=600°C; Leiten durch ein Nickel-Rohr;
参考文献
Severson; Brice
Journal of the American Chemical Society, 1958 , vol. 80, p. 2313,2316
反应条件
1: (FSO2O)2
2: ClOSO2F, HSO3F, SbF5
3: KF / bis-(2-methoxy-ethyl) ether
4: KF / bis-(2-methoxy-ethyl) ether
5: KF / bis-(2-methoxy-ethyl) ether
6: K2CO3 / bis-(2-methoxy-ethyl) ether
View Scheme
参考文献
Rapkin, A. I.; Zabolot-skikh, V. F.; Kochanov, A. S.; Tiunov, A. V.; Zhirnov, O. M.
Russian Journal of Applied Chemistry, 1995 , vol. 68, # 1part2 p. 133 - 134
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1995 , vol. 68, # 1 p. 151 - 152
