2,3-O-异亚丙基-D-核糖酸 gamma-内酯合成路线 (共 36 条)
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=0°C; 5 h;
参考文献
Bennis, Khalil; Calinaud, Pierre; Gelas, Jacques; Ghobsi, Mebrouk
Carbohydrate Research, 1994 , vol. 264, # 1 p. 33 - 44
反应条件
1: With hydrogenchloride in water T=20°C; 3 h; 2: With copper(II) sulfate in water T=60°C; 1.5 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 22 p. 7720 - 7726
反应条件
toluene-4-sulfonic acid T=25°C; 24 h;
参考文献
Tetrahedron, , vol. 53, # 4 p. 1311 - 1322
反应条件
1: With Amberlite IR-120H T=20°C; 18 h; 2: in water
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 22 p. 7720 - 7726
反应条件
1: With hydrogenchloride in water T=20°C; 3 h; 2: With copper(II) sulfate in water T=60°C; 4 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 22 p. 7720 - 7726
反应条件
hydrogenchloride 20 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 49, # 2 p. 349 - 362
反应条件
hydrogenchloride; acetone
参考文献
Canadian Journal of Chemistry, , vol. 36, p. 1720,1725
反应条件
sulfuric acid T=20°C; 48 h;
参考文献
Pinter
Polish Journal of Chemistry, 2005 , vol. 79, # 2 p. 323 - 328
反应条件
1.1: carbon-supported palladium-bismuth; oxygen; potassium hydroxide / water / 1.83 h / 50 °C / pH 9 2.1: hydrogenchloride / water / 3 h / 20 °C 2.2: 1.5 h / 60 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 22 p. 7720 - 7726
反应条件
1: 55.4 percent / Br2 / H2O 2: 48.5 percent / H2SO4 / 48 h / 20 °C View Scheme
参考文献
Polish Journal of Chemistry, , vol. 79, # 2 p. 323 - 328