3,5-二硝基-2-氨基吡啶合成路线 （共 24 条）
参考文献
Chemische Berichte, , vol. 61, p. 1230
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 60, p. 975
Chemische Berichte, , vol. 58, p. 1209
Chemische Berichte, , vol. 58, p. 1706
Chemische Berichte, , vol. 59, p. 2048
参考文献
Chemische Berichte, , vol. 61, p. 1230
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 60, p. 975
反应条件
potassium permanganate; ammonia T=-33°C; 1 h; Yields of byproduct given;
参考文献
Wozniak, Marian; Baranski, Andrzej; Szpakiewicz, Barbara
Liebigs Annalen der Chemie, 1993 , # 1 p. 7 - 10
反应条件
hydrogen fluoride; boric acid
参考文献
Wandas; Talik
Journal of Molecular Structure, 2013 , vol. 1043, p. 15 - 27
反应条件
(NH4)2S in methanol; water T=75°C;
参考文献
Newhouse, Bradley J.; Wenglowsky, Steve; Grina, Jonas; Laird, Ellen R.; Voegtli, Walter C.; Ren, Li; Ahrendt, Kateri; Buckmelter, Alex; Gloor, Susan L.; Klopfenstein, Nathalie; Rudolph, Joachim; Wen, Zhaoyang; Li, Xianfeng; Feng, Bainian
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 21 p. 5896 - 5899
参考文献
Sircar, Jagadish C.; Thomas, Richard J.; Richards, Mark L.; Sinha, Anjana
Patent: US2004/116466 A1, 2004 ;
反应条件
1: (NH4)2S / water; methanol / |Reflux 2: trichlorophosphate / |Reflux 3: ammonium chloride; zinc / water; ethanol View Scheme
参考文献
Newhouse, Bradley J.; Wenglowsky, Steve; Grina, Jonas; Laird, Ellen R.; Voegtli, Walter C.; Ren, Li; Ahrendt, Kateri; Buckmelter, Alex; Gloor, Susan L.; Klopfenstein, Nathalie; Rudolph, Joachim; Wen, Zhaoyang; Li, Xianfeng; Feng, Bainian
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 21 p. 5896 - 5899
反应条件
1: (NH4)2S / water; methanol / |Reflux 2: trichlorophosphate / |Reflux View Scheme
参考文献
Newhouse, Bradley J.; Wenglowsky, Steve; Grina, Jonas; Laird, Ellen R.; Voegtli, Walter C.; Ren, Li; Ahrendt, Kateri; Buckmelter, Alex; Gloor, Susan L.; Klopfenstein, Nathalie; Rudolph, Joachim; Wen, Zhaoyang; Li, Xianfeng; Feng, Bainian
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 21 p. 5896 - 5899
反应条件
1: 80 percent / aq.(NH4)2S / methanol / 0.5 h / Heating 2: 74 percent / aq.HCl / 16 h / Heating View Scheme
参考文献
Cai, Sui Xiong; Huang, Jin-Cheng; Espitia, Stephen A.; Tran, Minhtam; Ilyin, Victor I.; Hawkinson, Jon E.; Woodward, Richard M.; Weber, Eckard; Keana, John F.W.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 22 p. 3679 - 3686
反应条件
1: (NH4)2S / water; methanol / |Reflux 2: trichlorophosphate / |Reflux 3: ammonium chloride; zinc / water; ethanol View Scheme
参考文献
Newhouse, Bradley J.; Wenglowsky, Steve; Grina, Jonas; Laird, Ellen R.; Voegtli, Walter C.; Ren, Li; Ahrendt, Kateri; Buckmelter, Alex; Gloor, Susan L.; Klopfenstein, Nathalie; Rudolph, Joachim; Wen, Zhaoyang; Li, Xianfeng; Feng, Bainian
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 21 p. 5896 - 5899
