3,5-二硝基-2-氨基吡啶合成路线 （共 24 条）
反应条件
1: (NH4)2S / water; methanol / |Reflux
2: trichlorophosphate / |Reflux
View Scheme
参考文献
Newhouse, Bradley J.; Wenglowsky, Steve; Grina, Jonas; Laird, Ellen R.; Voegtli, Walter C.; Ren, Li; Ahrendt, Kateri; Buckmelter, Alex; Gloor, Susan L.; Klopfenstein, Nathalie; Rudolph, Joachim; Wen, Zhaoyang; Li, Xianfeng; Feng, Bainian
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 21 p. 5896 - 5899
反应条件
1: (NH4)2S / water; methanol / |Reflux
2: trichlorophosphate / |Reflux
View Scheme
参考文献
Newhouse, Bradley J.; Wenglowsky, Steve; Grina, Jonas; Laird, Ellen R.; Voegtli, Walter C.; Ren, Li; Ahrendt, Kateri; Buckmelter, Alex; Gloor, Susan L.; Klopfenstein, Nathalie; Rudolph, Joachim; Wen, Zhaoyang; Li, Xianfeng; Feng, Bainian
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 21 p. 5896 - 5899
反应条件
potassium permanganate; ammonia
T=-33°C; 1 h; Yields of byproduct given;
参考文献
Wozniak, Marian; Baranski, Andrzej; Szpakiewicz, Barbara
Liebigs Annalen der Chemie, 1993 , # 1 p. 7 - 10
反应条件
1: liquid NH3, KMnO4 / 1 h / -33 °C
2: 7 percent / liquid NH3, KMnO4 / 1 h / -33 °C
View Scheme
参考文献
Wozniak, Marian; Baranski, Andrzej; Szpakiewicz, Barbara
Liebigs Annalen der Chemie, 1993 , # 1 p. 7 - 10
