6H-苯并[cd]芘-6-酮合成路线 （共 18 条）
反应条件
sulfuric acid Condensation; 4 h; Heating;
参考文献
Morgenthaler, Jens; Ruechardt, Christoph
European Journal of Organic Chemistry, 1999 , # 9 p. 2219 - 2230
反应条件
sodium dichromate T=250°C;
参考文献
Newman,M.S.; Boden,H.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1759 - 1761
反应条件
water; 2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene 1.5 h; Heating; Yield given;
参考文献
Tintel, C.; Brugge, M. van der; Lugtenburg, J.; Cornelisse, J.
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 4 p. 220 - 223
反应条件
1: Na / diethyl ether; liquid ammonia / 1 h / -78 °C 2: 2) 2 N H2SO4 / 1) Et2O, liq. NH3, -78 deg C, 12 h 3: 80 percent / polyphosphoric acid / CH2Cl2 / 1 h / 100 °C 4: NaBH4 / tetrahydrofuran; H2O / 2 h / Ambient temperature 5: SOCl2, pyridine / CHCl3 / 2 h / Heating 6: DDQ, H2O / toluene / 1.5 h / Heating View Scheme
参考文献
Tintel, C.; Brugge, M. van der; Lugtenburg, J.; Cornelisse, J.
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 4 p. 220 - 223
反应条件
1: NaBH4 / tetrahydrofuran; H2O / 2 h / Ambient temperature 2: SOCl2, pyridine / CHCl3 / 2 h / Heating 3: DDQ, H2O / toluene / 1.5 h / Heating View Scheme
参考文献
Tintel, C.; Brugge, M. van der; Lugtenburg, J.; Cornelisse, J.
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 4 p. 220 - 223
反应条件
1: SOCl2, pyridine / CHCl3 / 2 h / Heating 2: DDQ, H2O / toluene / 1.5 h / Heating View Scheme
参考文献
Tintel, C.; Brugge, M. van der; Lugtenburg, J.; Cornelisse, J.
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 4 p. 220 - 223
反应条件
1: 80 percent / polyphosphoric acid / CH2Cl2 / 1 h / 100 °C 2: NaBH4 / tetrahydrofuran; H2O / 2 h / Ambient temperature 3: SOCl2, pyridine / CHCl3 / 2 h / Heating 4: DDQ, H2O / toluene / 1.5 h / Heating View Scheme
参考文献
Tintel, C.; Brugge, M. van der; Lugtenburg, J.; Cornelisse, J.
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 4 p. 220 - 223
反应条件
sulfuric acid T=120 - 125°C;
参考文献
Vollmann et al.
Justus Liebigs Annalen der Chemie, 1937 , vol. 531, p. 1,155
参考文献
Scholl; Meyer
Chemische Berichte, 1936 , vol. 69, p. 152,157
Full Text Show Details
Vollmann et al.
Justus Liebigs Annalen der Chemie, 1937 , vol. 531, p. 1,56, 155
参考文献
Scholl; Meyer
Chemische Berichte, 1936 , vol. 69, p. 152,157
Full Text Show Details
Vollmann et al.
Justus Liebigs Annalen der Chemie, 1937 , vol. 531, p. 1,38
