11H-苯并[b]芴-11-酮合成路线 （共 42 条）
反应条件
1.1: n-BuLi / tetrahydrofuran / -78 °C 1.2: 0.25 h 2.1: MnO2 / CH2Cl2 / 20 °C 3.1: 61 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.08 h / 20 °C View Scheme
参考文献
Rodriguez, David; Navarro-Vazquez, Armando; Castedo, Luis; Dominguez, Domingo; Saa, Carlos
Tetrahedron Letters, 2002 , vol. 43, # 15 p. 2717 - 2720
反应条件
1.1: n-BuLi / tetrahydrofuran / -78 °C 1.2: 0.25 h 2.1: MnO2 / CH2Cl2 / 20 °C 3.1: 61 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.08 h / 20 °C View Scheme
参考文献
Rodriguez, David; Navarro-Vazquez, Armando; Castedo, Luis; Dominguez, Domingo; Saa, Carlos
Tetrahedron Letters, 2002 , vol. 43, # 15 p. 2717 - 2720
反应条件
1: IPy2BF4; tetrafluoroboric acid / dichloromethane; diethyl ether / 24 h / -70 °C 2: palladium diacetate; triphenylphosphine; triethylamine / water; N,N-dimethyl-formamide / 22 h / 130 °C / |Inert atmosphere View Scheme
参考文献
Sarkar, Satinath; Jana, Manoranjan; Narender, Tadigoppula
European Journal of Organic Chemistry, 2013 , # 29 p. 6491 - 6495
反应条件
1: palladium diacetate; potassium carbonate / water; N,N-dimethyl-formamide / 2 h / 20 °C 2: IPy2BF4; tetrafluoroboric acid / dichloromethane; diethyl ether / 24 h / -70 °C 3: palladium diacetate; triphenylphosphine; triethylamine / water; N,N-dimethyl-formamide / 22 h / 130 °C / |Inert atmosphere View Scheme
参考文献
Sarkar, Satinath; Jana, Manoranjan; Narender, Tadigoppula
European Journal of Organic Chemistry, 2013 , # 29 p. 6491 - 6495
反应条件
1: palladium diacetate; potassium carbonate / water; N,N-dimethyl-formamide / 2 h / 20 °C 2: IPy2BF4; tetrafluoroboric acid / dichloromethane; diethyl ether / 24 h / -70 °C 3: palladium diacetate; triphenylphosphine; triethylamine / water; N,N-dimethyl-formamide / 22 h / 130 °C / |Inert atmosphere View Scheme
参考文献
Sarkar, Satinath; Jana, Manoranjan; Narender, Tadigoppula
European Journal of Organic Chemistry, 2013 , # 29 p. 6491 - 6495
参考文献
Cook; Stephenson
Journal of the Chemical Society, 1949 , p. 842,846
参考文献
Brown,D.N. et al.
Journal of the Chemical Society, 1961 , p. 3873 - 3879
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Baddar et al.
Journal of the Chemical Society, 1959 , p. 1009,1012
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Huisgen; Rist
Justus Liebigs Annalen der Chemie, 1955 , vol. 594, p. 137,153
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Huisgen; Zirngibl
Chemische Berichte, 1958 , vol. 91, p. 1438,1451
参考文献
Baddar et al.
Journal of the Chemical Society, 1959 , p. 1009,1012
反应条件
1: AlCl3; nitrobenzene 2: copper-powder; quinoline View Scheme
参考文献
Baddar et al.
Journal of the Chemical Society, 1959 , p. 1009,1012
反应条件
1: dipotassium peroxodisulfate; palladium diacetate; trifluoroacetic acid / 15 h / 120 °C / Inert atmosphere 2: hydrogenchloride; water / 100 °C / Inert atmosphere View Scheme
参考文献
Thirunavukkarasu, Vedhagiri S.; Cheng, Chien-Hong
Chemistry - A European Journal, 2011 , vol. 17, # 52 p. 14723 - 14726
