6,7-二甲氧基-1,2,3,4-四氢-异喹啉-3-羧酸盐酸盐合成路线 （共 5 条）
反应条件
hydrogenchloride in water 1) 3h, 90 deg C, 2) 0 deg C, 16h;
参考文献
O'Reilly; Derwin; Lin
Synthesis, 1990 , # 7 p. 550 - 556
反应条件
1: 84 percent / Na2CO3 2: 95 percent / H2 / 10percent Pd-C / methanol / 72 h / 760 Torr 3: 93 percent / conc. HCl / H2O / 20 h / Heating 4: 100 percent / conc. HCl / H2O / 1) 3h, 90 deg C, 2) 0 deg C, 16h View Scheme
参考文献
O'Reilly; Derwin; Lin
Synthesis, 1990 , # 7 p. 550 - 556
反应条件
1: 95 percent / H2 / 10percent Pd-C / methanol / 72 h / 760 Torr 2: 93 percent / conc. HCl / H2O / 20 h / Heating 3: 100 percent / conc. HCl / H2O / 1) 3h, 90 deg C, 2) 0 deg C, 16h View Scheme
参考文献
O'Reilly; Derwin; Lin
Synthesis, 1990 , # 7 p. 550 - 556
反应条件
1: 68 percent / acetic anhydride / Heating 2: 84 percent / Na2CO3 3: 95 percent / H2 / 10percent Pd-C / methanol / 72 h / 760 Torr 4: 93 percent / conc. HCl / H2O / 20 h / Heating 5: 100 percent / conc. HCl / H2O / 1) 3h, 90 deg C, 2) 0 deg C, 16h View Scheme
参考文献
O'Reilly; Derwin; Lin
Synthesis, 1990 , # 7 p. 550 - 556
反应条件
1: 93 percent / conc. HCl / H2O / 20 h / Heating 2: 100 percent / conc. HCl / H2O / 1) 3h, 90 deg C, 2) 0 deg C, 16h View Scheme
参考文献
O'Reilly; Derwin; Lin
Synthesis, 1990 , # 7 p. 550 - 556
