2,2’,5,5’-四甲基联苯基合成路线 （共 11 条）
反应条件
potassium phosphate; 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane; tris(dibenzylideneacetone)dipalladium (0) in 1,4-dioxane T=110°C; 15 h;
参考文献
Billingsley, Kelvin L.; Barder, Timothy E.; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 28 p. 5359 - 5363
反应条件
Ag2CO3; oxygen; palladium diacetate in dimethyl sulfoxide T=130°C; 12 h; Sealed tube; Reagent/catalystSolventTemperatureTime;
参考文献
Luo, Hai-Qing; Dong, Wen; Loh, Teck-Peng
Tetrahedron Letters, 2013 , vol. 54, # 22 p. 2833 - 2836
反应条件
[2,2']bipyridinyl; sodium bromide; nickel dichloride; zinc in N,N-dimethyl-formamide T=60 - 80°C; 4 h;
参考文献
Adonin; Ryabinin; Starichenko
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 2 p. 286 - 287
反应条件
sodium hydroxide; hydrazine hydrate; mercury dichloride; palladium dichloride 6 h; Heating;
参考文献
Nakajima, Riichiro; Shintani, Yuji; Hara, Tadashi
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 6 p. 1767 - 1768
反应条件
[bis(acetoxy)iodo]benzene; hydrogen tetrachloroaurate(III) in acetic acid T=55°C; 17 h;
参考文献
Kar, Anirban; Mangu, Naveenkumar; Kaiser, Hanns Martin; Beller, Matthias; Tse, Man Kin
Chemical Communications, 2008 , # 3 p. 386 - 388
反应条件
potassium phosphate; t-butylmethylbenzyl sulfide; phenyl halide; palladium dichloride in N,N-dimethyl-formamide T=100°C; 115 h;
参考文献
Tetrahedron Letters, , vol. 43, # 13 p. 2327 - 2329
反应条件
gold(III) chloride in 1,2-dichloro-ethane T=110°C;
参考文献
Organic Letters, , vol. 13, # 19 p. 4988 - 4991
反应条件
hydrogen tetrachloroaurate(III); [bis(acetoxy)iodo]benzene in acetic acid T=55°C; 17 h;
参考文献
Kar, Anirban; Mangu, Naveenkumar; Kaiser, Hanns Martin; Tse, Man Kin
Journal of Organometallic Chemistry, 2009 , vol. 694, # 4 p. 524 - 537
反应条件
gold(III) chloride; acetic acid T=55°C; 17 h;
参考文献
Organic Letters, , vol. 13, # 19 p. 4988 - 4991
反应条件
palladium diacetate in trifluoroacetic acid T=90°C; 6 h; in presence of K4H<CoW12O40>; velocities related to benzene reactivity toward biaryl formation; MechanismRate constant;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 20 p. 1392 - 1394
