反应条件
mercury(II) diacetate in chloroform addn. of B-compd. to stirred mixt. of Pb-compd. and Hg-compd. in CHCl3 over 15 min (40°C), stirring (40°C, 1 h and room temp. overnight); filtration (Celite), washing of filtrate (H2O), extn. of aq. layer (CHCl3), filtration of combined org. layer (Celite), concn. 40°C), addn. of petroleum ether, standing (0°C, overnight);
参考文献
Morgan, Jacqueline; Pinhey, John T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 715 - 720
