1: Hunigs base / methanol / 1.5 h 2: SOCl2, Et3N / CH2Cl2 / 18 h / 25 °C 3: 99 percent / Et3N, (CH3)2N(C6H4N) / CH2Cl2 / 2 h / 25 °C 4: 95 percent Spectr. / K2CO3 / tetrahydrofuran; H2O / 15 h 5: 83 percent View Scheme

暂无反应条件数据

2: 90 percent / EDCI, HOBt, / tetrahydrofuran; dimethylformamide / 14 h / 25 °C View Scheme