菲并[4,5-bcd]噻吩合成路线 （共 7 条）
反应条件
hydrogen sulfide; Harshaw Cr-0101T catalyst T=530°C;
参考文献
Klemm, L. H.; Tsuchiya, Reiko; Wong, Eric K. L.; Stevens, Michael P.; Lu, Jennifer J.; Klopfenstein, C. E.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 357 - 360
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 2 h; Ambient temperature;
参考文献
Klemm, L. H.; Tsuchiya, Reiko; Wong, Eric K. L.; Stevens, Michael P.; Lu, Jennifer J.; Klopfenstein, C. E.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 357 - 360
反应条件
polyphoshoric acid T=130 - 140°C; 2 h;
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1149 - 1152
反应条件
hydrogen sulfide; Harshaw Cr-0101 catalyst in benzene T=550°C; Product distribution;
参考文献
Klemm, L. H.; Pou, Sovitj; Detlefsen, W. D.; Higgins, Clay; Lawrence, Ross F.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 1293 - 1296
反应条件
hydrogen sulfide; Harshaw Cr-0101 T catalyst in benzene T=550°C; Product distribution;
参考文献
Klemm, L. H.; Pou, Sovitj; Detlefsen, W. D.; Higgins, Clay; Lawrence, Ross F.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 1293 - 1296
反应条件
methanol; hydrogen sulfide T=550°C; 2 h; object of study: sulfur bridging reaction vs. hydrodehalogenation; MechanismProduct distribution;
参考文献
Klemm, L. H.; Stevens, Michael P.; Tran, Long K.; Sheley, John
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 1111 - 1116
反应条件
1: 90percent HNO3 (d 1.44 g/ml), acetic anhydride / Ambient temperature; overnight
2: 93 percent / Fe, acetic acid / 0.5 h / 80 - 90 °C
3: 50 mg / W-2 Raney nickel / ethanol / 48 h / Heating
View Scheme
参考文献
Klemm, L. H.; Tsuchiya, Reiko; Wong, Eric K. L.; Stevens, Michael P.; Lu, Jennifer J.; Klopfenstein, C. E.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 357 - 360
