AC-ALA-ALA-OME合成路线 （共 7 条）
反应条件
glyceroacetonide-oxyma; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in water T=20°C; 2 h; optical yield given as percent de;
参考文献
Wang, Qinghui; Wang, Yong; Kurosu, Michio
Organic Letters, 2012 , vol. 14, # 13 p. 3372 - 3375
反应条件
1: 100 percent / 2 N HCl, H2 / Pd / methanol 2: 90 percent / pyridine / 3 h / Ambient temperature View Scheme
参考文献
Jahreis, Guenther; Fittkau, Siegfried
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 1 p. 35 - 40
反应条件
triethylamine in tetrahydrofuran; N,N-dimethyl-formamide T=15°C; 1 h; Yield given;
参考文献
Jahreis, Guenther; Fittkau, Siegfried
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 1 p. 35 - 40
反应条件
in pyridine 3 h; Ambient temperature;
参考文献
Jahreis, Guenther; Fittkau, Siegfried
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 1 p. 35 - 40
反应条件
1: HCl, i-amylnitrite / tetrahydrofuran; dimethylformamide / 0.25 h / -15 °C 2: NEt3 / tetrahydrofuran; dimethylformamide / 1 h / 15 °C View Scheme
参考文献
Jahreis, Guenther; Fittkau, Siegfried
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 1 p. 35 - 40
反应条件
1: 55 °C / thermitase, H2O, pH 8.0 2: 67 percent / NEt3, ethyl chlorocarbonate / tetrahydrofuran; dimethylformamide / 1.) -10 deg C, pH 7.5, 1 h; 2.) 4 deg C, overnight View Scheme
参考文献
Jahreis, Guenther; Fittkau, Siegfried
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 1 p. 35 - 40
反应条件
4-(N,N-dimethlyamino)pyridine; sodium hydroxide in pyridine
Ambient temperature;
参考文献
Jahreis, Guenther; Fittkau, Siegfried
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 1 p. 35 - 40
