(S)-(-)-1-(2-萘基)乙胺合成路线 （共 21 条）
反应条件
1: diphenylphosphoryl azide / toluene / 16 h / 20 °C 2: 961 mg / LiAlH4 / diethyl ether / a) reflux, 2 h, b) 20 deg C, 12 h View Scheme
参考文献
Tetrahedron, , vol. 52, # 12 p. 4199 - 4214
反应条件
samarium diiodide; hydrogen; 1.) <(COD)Rh(1,2-bis((2R,5R)-2,5-diethylphospholano)-benzene)>+CF3SO3- 1.) 0 deg C, 12 h, isopropanol, 60 psi; 2.) methanol, THF, 30 min; Multistep reaction. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 50, # 15 p. 4399 - 4428
参考文献
Diss. <Lund 1923> S.65
反应条件
sodium hydroxide; bromine
参考文献
Tetrahedron, , vol. 35, p. 1301 - 1306
反应条件
1: (i) SOCl2, (ii) aq. NH3 2: Br2, aq. NaOH View Scheme
参考文献
Tetrahedron, , vol. 35, p. 1301 - 1306
反应条件
sodium tetrahydroborate; (S)-valinol; zirconium tetrachloride 1) THF, r.t., 2) THF, r.t.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1548 - 1549
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemical Communications, , # 2 p. 173 - 174
反应条件
Ni T=110°C; 2 h; Inert atmosphere;
参考文献
Geukens, Inge; Plessers, Eva; Seo, Jin Won; De Vos, Dirk E.
European Journal of Inorganic Chemistry, 2013 , # 14 p. 2623 - 2628
反应条件
Ni T=110°C; 2 h; Inert atmosphere;
参考文献
Geukens, Inge; Plessers, Eva; Seo, Jin Won; De Vos, Dirk E.
European Journal of Inorganic Chemistry, 2013 , # 14 p. 2623 - 2628
反应条件
Ni T=110°C; 2 h; Inert atmosphere;
参考文献
Geukens, Inge; Plessers, Eva; Seo, Jin Won; De Vos, Dirk E.
European Journal of Inorganic Chemistry, 2013 , # 14 p. 2623 - 2628
