1-甲基-4-苯基-5-氨基吡唑合成路线 (共 3 条)
反应条件
1: thionyl chloride / benzene / 2 h / Heating 2: hydroxyl amine hydrochloride, aq. NaOH / diethyl ether / 3 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 31, # 6 p. 316 - 321
反应条件
1: aq. NaOH / ethanol 2: thionyl chloride / benzene / 2 h / Heating 3: hydroxyl amine hydrochloride, aq. NaOH / diethyl ether / 3 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 31, # 6 p. 316 - 321
反应条件
1: 1.) NaH / 1.) dioxane, 50 deg C, 2.) dioxane, 50 deg C, overnight 2: aq. NaOH / ethanol 3: thionyl chloride / benzene / 2 h / Heating 4: hydroxyl amine hydrochloride, aq. NaOH / diethyl ether / 3 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 31, # 6 p. 316 - 321