4-乙酰氨基苯基-三乙酰基-beta-D-葡萄糖苷酸甲酯合成路线 (共 8 条)
反应条件
1: in dichloromethane 0.5 h; Molecular sieve; 2: With boron trifluoride diethyl etherate in dichloromethane T=0°C;
参考文献
Hayes, John A.; Eccles, Kevin S.; Lawrence, Simon E.; Moynihan, Humphrey A.
Carbohydrate Research, 2012 , vol. 349, p. 108 - 112
反应条件
1: pyridine 2: acetone; silver oxide View Scheme
参考文献
Biochemical Journal, , vol. 42, p. 538,541
Biochemical Journal, , vol. 44, p. 242,245, 250, 251
反应条件
acetone; silver(l) oxide
参考文献
Biochemical Journal, , vol. 42, p. 538,541
Biochemical Journal, , vol. 44, p. 242,245, 250, 251
反应条件
aluminium amalgam 1.) ether, ethyl acetate, 15-20 deg C, 5 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Medicinal Chemistry, , vol. 24, # 8 p. 988 - 993
反应条件
pyridine; diethyl ether; ethanol Reaktion ueber zwei Stufen;
参考文献
Biochemical Journal, , vol. 42, p. 538,541
Biochemical Journal, , vol. 44, p. 242,245, 250, 251
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 40, # 7 p. 1852 - 1859
反应条件
1: With water in tetrahydrofuran; methanol T=0°C; Inert atmosphere; 2: With potassium carbonate in tetrahydrofuran; methanol T=40°C; 5 h; Inert atmosphere; Further stages;
参考文献
Hayes, John A.; Eccles, Kevin S.; Lawrence, Simon E.; Moynihan, Humphrey A.
Carbohydrate Research, 2012 , vol. 349, p. 108 - 112
反应条件
1: With water in tetrahydrofuran; methanol T=0°C; Inert atmosphere; 2: With potassium carbonate in tetrahydrofuran; methanol T=40°C; 5 h; Inert atmosphere; 3: in tetrahydrofuran; methanol; water T=20°C; Inert atmosphere;
参考文献
Hayes, John A.; Eccles, Kevin S.; Lawrence, Simon E.; Moynihan, Humphrey A.
Carbohydrate Research, 2012 , vol. 349, p. 108 - 112