1,3-二乙基-1,3-二嗪农-2-酮合成路线 (共 6 条)
反应条件
ClAu(di(tert-butyl)(1,1′-biphenyl-2-yl)-phosphine); silver trifluoromethanesulfonate in 1,4-dioxane T=100°C; P=6205.94 Torr; 19 h; Autoclave;
参考文献
Zhang, Zhibin; Lee, Seong Du; Widenhoefer, Ross A.
Journal of the American Chemical Society, 2009 , vol. 131, p. 5372 - 5373
反应条件
1: With selenium T=20°C; P=750.075 Torr; 2 h; neat (no solvent); 2: With oxygen T=20°C; P=750.075 Torr; 1 h; neat (no solvent);
参考文献
Mizuno, Takumi; Nakai, Takeo; Mihara, Masatoshi
Synthesis, 2010 , # 24 art. no. F15510SS, p. 4251 - 4255
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride 5 h; Heating;
参考文献
Bogat-skii, A. V.; Luk'yanenko, N. G.; Kirichenko, T. I.; Limich, V. V.; Karpenko, L. P.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 1 p. 89 - 95
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 1 p. 101 - 108
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US4918186 A1, 1990 ;
反应条件
sodium hydride 1.) dioxane, 1.5 h, rfx, 2.) 3.5 h, rfx; Yield given. Multistep reaction;
参考文献
Li, Chau-der; Mella, Sharon L.; Sartorelli, Alan C.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 9 p. 1089 - 1092
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride 5 h; Heating;
参考文献
Bogatsky, A. V.; Lukyanenko, N. G.; Kirichenko, T. I.
Synthesis, 1982 , # 6 p. 464 - 465