1,1,4,7,10,10-六甲基三亚乙基四胺合成路线 （共 10 条）
反应条件
formic acid 24 h; Heating;
参考文献
Che, Chi-Ming; Tang, Wai-Tong; Lam, Michael Hon-Wah; Mak, Thomas C. W.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 2885 - 2888
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Zhurnal Organicheskoi Khimii, , vol. 2, p. 1261 - 1265,1257 - 1260
反应条件
in benzene-d6 stirred for a few min, left standing in NMR tube at 22°C for several h; reversible reaction; not isolated; (1)H NMR spectral data;
参考文献
Organometallics, , vol. 19, # 23 p. 4810 - 4819
反应条件
in benzene-d6 stirred for a few min, left standing in NMR tube at 22°C for several h; reversible reaction; not isolated; (1)H NMR spectral data;
参考文献
Organometallics, , vol. 19, # 23 p. 4810 - 4819
反应条件
in benzene-d6 stirred for a few min, left standing in NMR tube at 22°C for several h; reversible reaction; not isolated; (1)H NMR spectral data;
参考文献
Organometallics, , vol. 19, # 23 p. 4810 - 4819
反应条件
hydrogenchloride 1.) reflux, 8 h; Multistep reaction;
参考文献
Journal of Physical Chemistry, , vol. 85, # 1 p. 64 - 68
参考文献
FMC Corporation
Patent: US4254050 A1, 1981 ;
Title/Abstract Full Text Show Details
FMC Corporation
Patent: US4322534 A1, 1982 ;
反应条件
in benzene-d6 stirred for a few min, left standing in NMR tube at 22°C for several h; reversible reaction; not isolated; (1)H NMR spectral data;
参考文献
Tang, Hui
Organometallics, 2000 , vol. 19, # 23 p. 4810 - 4819
反应条件
in benzene-d6 stirred for a few min, left standing in NMR tube at 22°C for several h; reversible reaction; not isolated; (1)H NMR spectral data;
参考文献
Tang, Hui
Organometallics, 2000 , vol. 19, # 23 p. 4810 - 4819
反应条件
n-butyllithium in pentane
a) 0 deg C, 1 h, b) RT, 1 h;
参考文献
Luitjes; Schakel; Klumpp
Synthetic Communications, 1994 , vol. 24, # 16 p. 2257 - 2261
