反应条件
Multi-step reaction with 3 steps 1: 1.) NaH / 1.) THF, RT, 30 min, 2.) THF, reflux, 24 h2: 95 percent / m-CPBA / CH2Cl2 / -78 °C3: 1.) LDA, HMPT / 1.) THF, hexane, -35 deg C, 3 h, 2.) THF, hexane, from -35 deg C to RT, 2 h
参考文献
Avery; Chong; Jennings-White Journal of the American Chemical Society, 1992 , vol. 114, # 3 p. 974 - 979
