Houlden, Chris E.; Bailey, Chris D.; Ford, J. Gair; Gagne, Michel R.; Lloyd-Jones, Guy C.; Booker-Milburn, Kevin I.
Journal of the American Chemical Society, 2008 , vol. 130, # 31 p. 10066 - 10067
diisopropylamine; trichlorophosphate in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Polisar, Jason G.; Norton, Jack R.
Tetrahedron, 2012 , vol. 68, # 49 p. 10236 - 10240,5
Title/Abstract Show Details
Polisar, Jason G.; Norton, Jack R.
Tetrahedron, 2012 , vol. 68, # 49 p. 10236 - 10240
1: 57 percent / Na / dimethylformamide; toluene / 2 h / 150 - 155 °C
2: 31 percent / sodium borohydride / Palladium-charcoal (5percent) / methanol; H2O / Ambient temperature
View Scheme
参考文献
Cadogan, J. I. G.; Hutchison, H. Susan; McNab, Hamish
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1407 - 1412
dichlorotris(triphenylphosphine)ruthenium(II) in 1,3,5-trimethyl-benzene
12 h; Heating;
参考文献
Kotachi, Shinji; Tsuji, Yasushi; Kondo, Teruyuki; Watanabe, Yoshihisa
Journal of the Chemical Society, Chemical Communications, 1990 , # 7 p. 549 - 550
sodium in N,N-dimethyl-formamide; toluene
T=150 - 155°C; 2 h;
参考文献
Cadogan, J. I. G.; Hutchison, H. Susan; McNab, Hamish
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1407 - 1412