3,4,5-三甲氧基苯甲酰胺合成路线 （共 33 条）
反应条件
1: phosphorus pentachloride; benzene 2: diethyl ether; benzene View Scheme
参考文献
Harding
Journal of the Chemical Society, 1914 , vol. 105, p. 2794
参考文献
Heffter; Capellmann
Chemische Berichte, 1905 , vol. 38, p. 3636
反应条件
NaClO; sodium hydroxide in water T=20 - 100°C;
参考文献
Qin, Qi-Xue; Yang, Jian; Chen, Duo-Zhi; Yang, Bo; Zhang, Ji
Organic Preparations and Procedures International, 2013 , vol. 45, # 4 p. 321 - 324
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 21, p. 1545
反应条件
1: hypochlorite; sodium hydroxide / unter Eiszusatz
2: Acetylierung
View Scheme
参考文献
Graebe; Suter
Justus Liebigs Annalen der Chemie, 1905 , vol. 340, p. 230
反应条件
copper(l) chloride in chlorobenzene
T=130°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Xia, Qinqin; Liu, Xiaolong; Zhang, Yuejiao; Chen, Chao; Chen, Wanzhi
Organic Letters, 2013 , vol. 15, # 13 p. 3326 - 3329
参考文献
Couturier
Annales de Chimie (Cachan, France), 1938 , vol. <11> 10, p. 559,597
反应条件
diphosphorus pentasulfide; sodium hydroxide in water; benzene
参考文献
Otsuka Pharmaceutical Co., Ltd.
Patent: US5643932 A1, 1997 ;
参考文献
Kowa Co., Ltd.
Patent: US6472386 B1, 2002 ;
反应条件
1: phosphorus pentachloride; benzene
2: diethyl ether; benzene
3: glacial acetic acid; concentrated nitric acid
View Scheme
参考文献
Harding
Journal of the Chemical Society, 1914 , vol. 105, p. 2794
