4-甲氧基-6-甲基-7,8-二氢[1,3]二氧杂环戊并[4,5-g]异喹啉-6-鎓碘化物合成路线 （共 14 条）
反应条件
iodine; potassium acetate in ethanol T=80°C; 3 h;
参考文献
Mao, Yongjun; Song, Shuai; Zhao, Dongmei; Cheng, Maosheng
Heterocycles, 2013 , vol. 87, # 12 p. 2633 - 2640
反应条件
1: 98 percent / H2 / 5percent Pd-C / ethanol 2: 99 percent / H2 / 5percent Pd-C / ethanol 3: 78 percent / 6N HCl 4: 99 percent / CH2Cl2 / 1 h / Ambient temperature 5: 95 percent / H2 / 5percent Pd-C / ethanol / 7 h / 50 °C 6: I2, potassium acetate / ethanol / 3 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 55, # 12 p. 3767 - 3771
反应条件
1: 99 percent / CH2Cl2 / 1 h / Ambient temperature 2: 95 percent / H2 / 5percent Pd-C / ethanol / 7 h / 50 °C 3: I2, potassium acetate / ethanol / 3 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 55, # 12 p. 3767 - 3771
反应条件
1: 99 percent / H2 / 5percent Pd-C / ethanol 2: 78 percent / 6N HCl 3: 99 percent / CH2Cl2 / 1 h / Ambient temperature 4: 95 percent / H2 / 5percent Pd-C / ethanol / 7 h / 50 °C 5: I2, potassium acetate / ethanol / 3 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 55, # 12 p. 3767 - 3771
反应条件
1: 95 percent / H2 / 5percent Pd-C / ethanol / 7 h / 50 °C 2: I2, potassium acetate / ethanol / 3 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 55, # 12 p. 3767 - 3771
反应条件
1: 78 percent / 6N HCl 2: 99 percent / CH2Cl2 / 1 h / Ambient temperature 3: 95 percent / H2 / 5percent Pd-C / ethanol / 7 h / 50 °C 4: I2, potassium acetate / ethanol / 3 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 55, # 12 p. 3767 - 3771
参考文献
Fleischhacker, Wilhelm; Richter, Bernd; Urban, Ernst
Monatshefte fuer Chemie, 1989 , vol. 120, p. 765 - 770
反应条件
1: 92 percent / KMnO4 / tetrahydrofuran / 0.42 h 2: 98 percent / ethanol View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 120, p. 765 - 770
反应条件
1.1: methanol; water / 1 h / 0 - 20 °C 1.2: 2 h / 0 - 20 °C 2.1: hydrogenchloride / water / 24 h / 20 °C 3.1: sodium tetrahydroborate; trifluoroacetic acid / dichloromethane / 25 h / 0 - 20 °C 4.1: iodine; potassium acetate / ethanol / 3 h / 80 °C View Scheme
参考文献
Heterocycles, , vol. 87, # 12 p. 2633 - 2640
反应条件
1: hydrogenchloride / water / 24 h / 20 °C 2: sodium tetrahydroborate; trifluoroacetic acid / dichloromethane / 25 h / 0 - 20 °C 3: iodine; potassium acetate / ethanol / 3 h / 80 °C View Scheme
参考文献
Heterocycles, , vol. 87, # 12 p. 2633 - 2640
