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乙二醇
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63148-62-9
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3095-33-8
合成路线
（共 30 条）
2025-95-8
1,8-双(溴甲基)萘
+
153725-04-3
→
反应条件
3095-33-8
反应条件
water in N,N-dimethyl-formamide T=152°C; 2 h; Inert atmosphere;
参考文献
Owsianik, Krzysztof; Vendier, Laure; Blaszczyk, Jaroslaw; Sieron, Leslaw
Tetrahedron, 2013 , vol. 69, # 5 p. 1628 - 1633
90-11-9
1-溴代萘
+
4559-70-0
二苯基磷氧
→
反应条件
3095-33-8
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100°C; Inert atmosphere;
参考文献
Zhao, Yu-Long; Wu, Guo-Jie; Li, You; Gao, Lian-Xun; Han, Fu-She
Chemistry - A European Journal, 2012 , vol. 18, # 31 p. 9622 - 9627
4559-70-0
二苯基磷氧
+
90-13-1
α-氯代萘
→
反应条件
3095-33-8
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=120°C; Inert atmosphere;
参考文献
Zhao, Yu-Long; Wu, Guo-Jie; Li, You; Gao, Lian-Xun; Han, Fu-She
Chemistry - A European Journal, 2012 , vol. 18, # 31 p. 9622 - 9627
68211-49-4
+
4559-70-0
二苯基磷氧
→
反应条件
3095-33-8
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; N-ethyl-N,N-diisopropylamine; zinc in N,N-dimethyl-formamide T=140°C; 36 h; Inert atmosphere;
参考文献
Shen, Chaoren; Yang, Guoqiang; Zhang, Wanbin
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 17 p. 3500 - 3505
1162-90-9
→
反应条件
3095-33-8
反应条件
dihydrogen peroxide in dichloromethane Yield given;
参考文献
Zhang, Hong-Yu; Yi, Hong-Ming; Wang, Gang-Wei; Yang, Bin; Yang, Shang-Dong
Organic Letters, 2013 , vol. 15, # 24 p. 6186 - 6189
90-15-3
1-萘酚
+
4559-70-0
二苯基磷氧
→
反应条件
3095-33-8
反应条件
1: α-naphthol With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in acetonitrile T=100°C; 3 h; Inert atmosphere; 2: diphenylphosphine oxide With [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in acetonitrile T=100°C; 18 h; Inert atmosphere;
参考文献
Zhao, Yu-Long; Wu, Guo-Jie; Han, Fu-She
Chemical Communications, 2012 , vol. 48, # 47 p. 5868 - 5870
33397-22-7
+
4559-70-0
二苯基磷氧
→
反应条件
3095-33-8
反应条件
pyridine; [2,2']bipyridinyl; palladium dichloride in toluene T=100°C; 24 h; Schlenk technique;
参考文献
Wang, Tao; Sang, Shuai; Liu, Liu; Qiao, Hongwei; Gao, Yuxing; Zhao, Yufen
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 608 - 617
→
反应条件
3095-33-8
反应条件
triethylamine; copper(l) chloride in dichloromethane T=20°C; 0.166667 h; Schlenk technique;
参考文献
Xu, Jian; Zhang, Pengbo; Gao, Yuzhen; Chen, Yiyin; Tang, Guo; Zhao, Yufen
Journal of Organic Chemistry, 2013 , vol. 78, # 16 p. 8176 - 8183
38262-42-9
+
4559-70-0
二苯基磷氧
→
反应条件
3095-33-8
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100°C; 18 h; Inert atmosphere;
参考文献
Zhao, Yu-Long; Wu, Guo-Jie; Han, Fu-She
Chemical Communications, 2012 , vol. 48, # 47 p. 5868 - 5870
90-11-9
1-溴代萘
+
829-85-6
二苯基膦
→
反应条件
1162-90-9
+
3095-33-8
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100°C; Inert atmosphere;
参考文献
Zhao, Yu-Long; Wu, Guo-Jie; Li, You; Gao, Lian-Xun; Han, Fu-She
Chemistry - A European Journal, 2012 , vol. 18, # 31 p. 9622 - 9627
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