2-羟基-2-(3-溴苯基)丙烷合成路线 （共 15 条）
反应条件
perchloric acid; hydrogen; palladium on activated charcoal in acetic acid
参考文献
Stiles,M.; Sisti,A.J.
Journal of Organic Chemistry, 1960 , vol. 25, # 10 p. 1691 - 1693
反应条件
1: phosphorus, aq. HI 2: (i) Mg, Et2O, (ii) /BRN= 1900390/, (iii) aq. HCl View Scheme
参考文献
Smith,J.G.; Turle,R.A.
Journal of Organic Chemistry, 1972 , vol. 37, # 1 p. 126 - 131
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium acetate in N,N-dimethyl-formamide T=120°C; 3 h;
参考文献
SANOFI; ARNAUD, Joëlle; ARTIAGA, Martine; BARTH, Francis; HORTALA, Laurent; MARTINEZ, Serge; ROUX, Pascale
Patent: WO2013/87643 A1, 2013 ;
Location in patent: Page/Page column 15-16 ;
反应条件
phosphorus; hydrogen iodide
参考文献
Smith,J.G.; Turle,R.A.
Journal of Organic Chemistry, 1972 , vol. 37, # 1 p. 126 - 131
反应条件
1: phosphorus, aq. HI 2: (i) Mg, Et2O, (ii) /BRN= 1900390/, (iii) aq. HCl 3: SOCl2 View Scheme
参考文献
Smith,J.G.; Turle,R.A.
Journal of Organic Chemistry, 1972 , vol. 37, # 1 p. 126 - 131
