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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-乙酰基-5-碘噻吩
合成路线
（共 27 条）
30955-94-3
2-乙酰基-5-碘噻吩
+
873-77-8
4-氯苯基溴化镁
→
反应条件
51335-90-1
1-[5-(4-氯苯基)-2-噻吩]-1-乙酮
+
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
2050-68-2
4,4'-二氯联苯
反应条件
1: 4-chlorophenyl-magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
+
544-92-3
氰化亚铜
→
反应条件
88653-55-8
2-乙酰基-5-氰基噻吩
反应条件
in pyridine 2.5 h; Heating;
参考文献
Jones, John R.; Pearson, Gerd M.; Spinelli, Domenico; Consiglio, Giovanni; Arnone, Caterina
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 557 - 558
30955-94-3
2-乙酰基-5-碘噻吩
+
873-77-8
4-氯苯基溴化镁
→
反应条件
51335-90-1
1-[5-(4-氯苯基)-2-噻吩]-1-乙酮
+
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
2050-68-2
4,4'-二氯联苯
反应条件
1: 4-chlorophenyl-magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Synlett, , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
+
36282-40-3
3-甲氧基苯基溴化镁
→
反应条件
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
6161-50-8
3,3-二甲氧基联苯
+
893735-15-4
反应条件
1: (3-methoxyphenyl)-magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
+
100-58-3
溴化苯基镁
→
反应条件
1665-41-4
1-(5-苯基噻吩-2-基)乙酮
+
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
92-52-4
联苯
反应条件
1: phenyl-magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
+
71-43-2
苯
→
反应条件
1665-41-4
1-(5-苯基噻吩-2-基)乙酮
反应条件
1 h; Irradiation;
参考文献
Antonioletti, Roberto; Auria, Maurizio D'; Onofrio, Franco D'; Piancatelli, Giovanni; Scettri, Arrigo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1755 - 1758
30955-94-3
2-乙酰基-5-碘噻吩
+
4294-57-9
对甲苯基溴化镁
→
反应条件
51335-91-2
+
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
613-33-2
4,4'-二甲基联苯
反应条件
1: (4-Methylphenyl)-magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
+
13139-86-1
3-甲基-CBS-氧硼啶
→
反应条件
13918-67-7
+
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
2132-80-1
4,4-二甲氧基联苯
反应条件
1: 4-methoxyphenyl magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
+
100-58-3
溴化苯基镁
→
反应条件
1665-41-4
1-(5-苯基噻吩-2-基)乙酮
+
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
92-52-4
联苯
反应条件
1: phenyl-magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
+
13139-86-1
3-甲基-CBS-氧硼啶
→
反应条件
13918-67-7
+
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
2132-80-1
4,4-二甲氧基联苯
反应条件
1: 4-methoxyphenyl magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
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