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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-乙酰基-5-碘噻吩
合成路线
（共 27 条）
30955-94-3
2-乙酰基-5-碘噻吩
+
4294-57-9
对甲苯基溴化镁
→
反应条件
51335-91-2
+
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
613-33-2
4,4'-二甲基联苯
反应条件
1: (4-Methylphenyl)-magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
+
36282-40-3
3-甲氧基苯基溴化镁
→
反应条件
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
6161-50-8
3,3-二甲氧基联苯
+
893735-15-4
反应条件
1: (3-methoxyphenyl)-magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
+
873-77-8
4-氯苯基溴化镁
→
反应条件
51335-90-1
1-[5-(4-氯苯基)-2-噻吩]-1-乙酮
+
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
2050-68-2
4,4'-二氯联苯
反应条件
1: 4-chlorophenyl-magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
+
352-13-6
4-氟苯基溴化镁
→
反应条件
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
886361-46-2
+
398-23-2
4,4'-二氟联苯
反应条件
1: (4-fluoro-phenyl)-magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
+
352-13-6
4-氟苯基溴化镁
→
反应条件
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
886361-46-2
+
398-23-2
4,4'-二氟联苯
反应条件
1: (4-fluoro-phenyl)-magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
→
反应条件
60166-85-0
5-碘-噻吩-2-羧酸
反应条件
sodium hydroxide; potassium permanganate; water
参考文献
Rinkes
Recueil des Travaux Chimiques des Pays-Bas, 1934 , vol. 53, p. 643,648
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 991
30955-94-3
2-乙酰基-5-碘噻吩
+
4294-57-9
对甲苯基溴化镁
→
反应条件
51335-91-2
+
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
613-33-2
4,4'-二甲基联苯
反应条件
1: (4-Methylphenyl)-magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
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