1,3-二甲基苯并咪唑-2-酮合成路线 (共 27 条)
反应条件
1: SOCl2 2: LiBH4; diethyl ether View Scheme
参考文献
Chemische Berichte, , vol. 91, p. 1432,1436
反应条件
T=165 - 185°C; 5 h; Yield given. Yields of byproduct given;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 21, # 12 p. 1398 - 1399
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 21, # 12 p. 1694 - 1695
反应条件
Neutral lead acetate T=159.85°C; 1 h;
参考文献
Fu, Yue; Baba, Toshihide; Ono, Yoshio
Journal of Catalysis, 2001 , vol. 197, # 1 p. 91 - 97
参考文献
Zhurnal Obshchei Khimii, , vol. 23, p. 1691,1694; engl. Ausg. S. 1779, 1781
Journal of the Chemical Society, , p. 2830,2831
反应条件
potassium hydroxide 5 h; Heatingother temperature; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 21, # 12 p. 1398 - 1399
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 21, # 12 p. 1694 - 1695
参考文献
Efros; El'zow
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 127,130; engl. Ausg. S. 143, 147
反应条件
aluminium trichloride
1) CH2Cl2, nitromethane, ice-bath; 2) CH2Cl2, nitromethane, rt, 1.5 h; Yield given. Multistep reaction;
参考文献
Petrov, Ognyan I.; Kalcheva, Veneta B.; Antonova, Antonina Ts.
Collection of Czechoslovak Chemical Communications, 1997 , vol. 62, # 3 p. 494 - 497