N6,N6,9-三-Boc-腺嘌呤合成路线 （共 2 条）
反应条件
sodium hydrogencarbonate in methanol; water T=50°C; Hydrolysis; 1 h;
参考文献
Dey; Garner
Journal of Organic Chemistry, 2000 , vol. 65, # 22 p. 7697 - 7699
反应条件
1.1: 93 percent / NaHCO3; H2O / methanol / 1.25 h / 50 °C
2.1: triphenylphosphine; DIAD / tetrahydrofuran / 0.67 h / 0 - 20 °C
2.2: 98 percent / tetrahydrofuran / 20 °C
3.1: 99 percent / TFA; MeOH / 1,2-dichloro-ethane / 20 °C
View Scheme
参考文献
Michel, Benoit Y.; Strazewski, Peter
Tetrahedron, 2007 , vol. 63, # 39 p. 9836 - 9841
