1,3-二氨基-4,6-二异丙基苯合成路线 （共 11 条）
反应条件
sodium tetrahydroborate; water; palladium on activated charcoal 1 h; Ambient temperature;
参考文献
Beak, Peter; Carter, Linda G.
Journal of Organic Chemistry, 1981 , vol. 46, # 11 p. 2363 - 2373
反应条件
nickel; isopropyl alcohol T=60°C; P=58840.6 Torr; Hydrogenation;
参考文献
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
反应条件
1: 64 percent / HNO3, CF3SO3H / CH2Cl2 / 1.) 25 deg C, 1 h, 2.) 30-38 deg C, 0.5 h 2: 86 percent / NaBH4, H2O / 10percent Pd/C / 1 h / Ambient temperature View Scheme
参考文献
Konishi, Hisatoshi; Hashimoto, Shun; Sakakibara, Terunobu; Matsubara, Shingo; Yasukawa, Yusuke; Morikawa, Osamu; Kobayashi, Kazuhiro
Tetrahedron Letters, 2009 , vol. 50, # 6 p. 620 - 623
反应条件
1: glacial acetic acid; acetic acid anhydride; HNO3 / 50 °C 2: Raney nickel; isopropyl alcohol / 100 °C / 58840.6 Torr / Hydrogenation 3: sulfuric acid; nitric acid 4: Raney nickel; isopropyl alcohol / 60 °C / 58840.6 Torr / Hydrogenation View Scheme
参考文献
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
反应条件
1: Raney nickel; isopropyl alcohol / 100 °C / 58840.6 Torr / Hydrogenation 2: sulfuric acid; nitric acid 3: Raney nickel; isopropyl alcohol / 60 °C / 58840.6 Torr / Hydrogenation View Scheme
参考文献
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
反应条件
1: glacial acetic acid; acetic acid anhydride; HNO3 / 30 - 45 °C 2: Raney nickel; isopropyl alcohol / 100 °C / 58840.6 Torr / Hydrogenation 3: sulfuric acid; nitric acid 4: Raney nickel; isopropyl alcohol / 60 °C / 58840.6 Torr / Hydrogenation View Scheme
参考文献
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
反应条件
1: Raney nickel; isopropyl alcohol / 100 °C / 58840.6 Torr / Hydrogenation 2: sulfuric acid; nitric acid 3: Raney nickel; isopropyl alcohol / 60 °C / 58840.6 Torr / Hydrogenation View Scheme
参考文献
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
反应条件
1: sulfuric acid; nitric acid 2: Raney nickel; isopropyl alcohol / 60 °C / 58840.6 Torr / Hydrogenation View Scheme
参考文献
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
反应条件
1: sulfuric acid; nitric acid 2: Raney nickel; isopropyl alcohol / 60 °C / 58840.6 Torr / Hydrogenation View Scheme
参考文献
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
反应条件
T=60°C; Hydrogenation;
参考文献
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
