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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
31031-05-7
合成路线
（共 6 条）
682802-82-0
6-苄氧基吲哚-3-乙酸
→
反应条件
31031-05-7
反应条件
hydrogen; palladium on activated charcoal in methanol Yield given;
参考文献
Shinada, Tetsuro; Miyachi, Miki; Itagaki, Yasuhiro; Naoki, Hideo; Yoshihara, Kazuo; Nakajima, Terumi
Tetrahedron Letters, 1996 , vol. 37, # 39 p. 7099 - 7102
610-81-1
3-硝基-4-氨基苯酚
→
反应条件
31031-05-7
反应条件
1: NaNO2, HCl 2: KI 3: 94 percent / K2CO3 / acetone 4: 92 percent / Pd(OAc)2, (Tol)3P, Et3N / acetonitrile / Heating 5: 98 percent / Zn, AcOH 6: 96 percent / pyridine / CH2Cl2 7: 92 percent / triphosgene, Et3N / CH2Cl2 8: 1.) Bu3SnH, AIBN; 2.) dil. HCl / 1.) MeCN, reflux; 2.) 0 deg C 9: NaOH / H2O; tetrahydrofuran 10: H2 / Pd-C / methanol View Scheme
参考文献
Shinada, Tetsuro; Miyachi, Miki; Itagaki, Yasuhiro; Naoki, Hideo; Yoshihara, Kazuo; Nakajima, Terumi
Tetrahedron Letters, 1996 , vol. 37, # 39 p. 7099 - 7102
113305-56-9
4-碘-3-硝基苯酚
→
反应条件
31031-05-7
反应条件
1: 94 percent / K2CO3 / acetone 2: 92 percent / Pd(OAc)2, (Tol)3P, Et3N / acetonitrile / Heating 3: 98 percent / Zn, AcOH 4: 96 percent / pyridine / CH2Cl2 5: 92 percent / triphosgene, Et3N / CH2Cl2 6: 1.) Bu3SnH, AIBN; 2.) dil. HCl / 1.) MeCN, reflux; 2.) 0 deg C 7: NaOH / H2O; tetrahydrofuran 8: H2 / Pd-C / methanol View Scheme
参考文献
Shinada, Tetsuro; Miyachi, Miki; Itagaki, Yasuhiro; Naoki, Hideo; Yoshihara, Kazuo; Nakajima, Terumi
Tetrahedron Letters, 1996 , vol. 37, # 39 p. 7099 - 7102
183007-32-1
→
反应条件
31031-05-7
反应条件
1: 92 percent / Pd(OAc)2, (Tol)3P, Et3N / acetonitrile / Heating 2: 98 percent / Zn, AcOH 3: 96 percent / pyridine / CH2Cl2 4: 92 percent / triphosgene, Et3N / CH2Cl2 5: 1.) Bu3SnH, AIBN; 2.) dil. HCl / 1.) MeCN, reflux; 2.) 0 deg C 6: NaOH / H2O; tetrahydrofuran 7: H2 / Pd-C / methanol View Scheme
参考文献
Shinada, Tetsuro; Miyachi, Miki; Itagaki, Yasuhiro; Naoki, Hideo; Yoshihara, Kazuo; Nakajima, Terumi
Tetrahedron Letters, 1996 , vol. 37, # 39 p. 7099 - 7102
183007-38-7
→
反应条件
31031-05-7
反应条件
1: NaOH / H2O; tetrahydrofuran 2: H2 / Pd-C / methanol View Scheme
参考文献
Shinada, Tetsuro; Miyachi, Miki; Itagaki, Yasuhiro; Naoki, Hideo; Yoshihara, Kazuo; Nakajima, Terumi
Tetrahedron Letters, 1996 , vol. 37, # 39 p. 7099 - 7102
31031-05-7
→
反应条件
443-31-2
6-羟基吲哚乙胺
反应条件
1: DIBAL / CH2Cl2 / -78 °C 2: pyridine / CH2Cl2 / 0 °C 3: NaN3 / dimethylformamide 4: H2 / 10percent Pd-C / methanol View Scheme
参考文献
Shinada, Tetsuro; Miyachi, Miki; Itagaki, Yasuhiro; Naoki, Hideo; Yoshihara, Kazuo; Nakajima, Terumi
Tetrahedron Letters, 1996 , vol. 37, # 39 p. 7099 - 7102
