3-(二甲氨基)-5,5-二甲基-2-环己烯-1-酮合成路线 （共 10 条）
反应条件
potassium carbonate; boron trifluoride diethyl etherate in dichloromethane; water 8 h; Ambient temperature;
参考文献
Kowalski, Conrad J.; Fields, Kevin W.
Journal of Organic Chemistry, 1981 , vol. 46, p. 197 - 201
反应条件
boron trifluoride diethyl etherate in benzene 6 h; Heating;
参考文献
Azzaro, Marcel; Geribaldi, Serge; Videau, Bruno
Synthesis, 1981 , # 11 p. 880 - 881
反应条件
1: 92 percent / potassium carbonate / CH2Cl2 / 2 h / Ambient temperature 2: 80 percent / potassium carbonate / boron trifluoride etherate / CH2Cl2; H2O / 8 h / Ambient temperature View Scheme
参考文献
Kowalski, Conrad J.; Fields, Kevin W.
Journal of Organic Chemistry, 1981 , vol. 46, p. 197 - 201
反应条件
in diethyl ether 96 h; Ambient temperature;
参考文献
Gompper, Rudolf; Kottmair, Eduard
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1990 , vol. 45, # 6 p. 833 - 847
参考文献
Shanazarov, A. K.; Granik, V. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 3 p. 359 - 360
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 3 p. 423 - 424
反应条件
sodium hydride 1.)dioxane,reflux,1 h 2.)2 eq iodomethane,reflux,1-2 h; Yield given. Multistep reaction;
参考文献
Greenhill, John V.; Moten, Ashraf M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3405 - 3408
反应条件
sodium hydride 1.) THF, reflux, 1 h, 2.) reflux, 2 h; Yield given. Multistep reaction;
参考文献
Greenhill, John V.; Moten, M. Ashraf; Hanke, Reiner
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 287 - 290
反应条件
sodium hydride in 1,4-dioxane HeatingEffect of solvents, ratio of reagents and reflux period. Other enaminones were also investigated.; Product distribution;
参考文献
Greenhill, John V.; Moten, Ashraf M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3405 - 3408
参考文献
Shanazarov, A. K.; Granik, V. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 3 p. 359 - 360
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 3 p. 423 - 424
反应条件
Lawesson's reagent in ethylene glycol dimethyl ether
参考文献
Boberg, Friedrich; Otten, Albert
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 112, # 1-4 p. 91 - 99
