1,4-二氢-5-甲基-4-氧代-吡咯并[2,1-f][1,2,4]三嗪-6-羧酸合成路线 (共 5 条)
反应条件
ethanol; sodium hydroxide T=60°C;
参考文献
Zheng, Bin; Conlon, David A.; Corbett, R. Michael; Chau, Melissa; Hsieh, Dau-Ming; Yeboah, Agnes; Hsieh, Daniel; Mueslehiddinoglu, Jale; Gallagher, William P.; Simon, Jeffrey N.; Burt, Justin
Organic Process Research and Development, 2012 , vol. 16, # 11 p. 1846 - 1853
反应条件
1: ethanol / 50 °C 2: ethanol; sodium ethanolate / 60 °C 3: potassium tert-butylate; O-(4-nitrobenzoyl) hydroxylamine / 1-methyl-pyrrolidin-2-one / 25 °C 4: phosphoric acid / 120 °C 5: ethanol; sodium hydroxide / 60 °C View Scheme
参考文献
Zheng, Bin; Conlon, David A.; Corbett, R. Michael; Chau, Melissa; Hsieh, Dau-Ming; Yeboah, Agnes; Hsieh, Daniel; Mueslehiddinoglu, Jale; Gallagher, William P.; Simon, Jeffrey N.; Burt, Justin
Organic Process Research and Development, 2012 , vol. 16, # 11 p. 1846 - 1853
反应条件
1: potassium tert-butylate; O-(4-nitrobenzoyl) hydroxylamine / 1-methyl-pyrrolidin-2-one / 25 °C 2: phosphoric acid / 120 °C 3: ethanol; sodium hydroxide / 60 °C View Scheme
参考文献
Zheng, Bin; Conlon, David A.; Corbett, R. Michael; Chau, Melissa; Hsieh, Dau-Ming; Yeboah, Agnes; Hsieh, Daniel; Mueslehiddinoglu, Jale; Gallagher, William P.; Simon, Jeffrey N.; Burt, Justin
Organic Process Research and Development, 2012 , vol. 16, # 11 p. 1846 - 1853
反应条件
1: phosphoric acid / 120 °C 2: ethanol; sodium hydroxide / 60 °C View Scheme
参考文献
Zheng, Bin; Conlon, David A.; Corbett, R. Michael; Chau, Melissa; Hsieh, Dau-Ming; Yeboah, Agnes; Hsieh, Daniel; Mueslehiddinoglu, Jale; Gallagher, William P.; Simon, Jeffrey N.; Burt, Justin
Organic Process Research and Development, 2012 , vol. 16, # 11 p. 1846 - 1853
反应条件
1: phosphoric acid / 125 °C 2: trichlorophosphate; N-ethyl-N,N-diisopropylamine / toluene / 100 °C View Scheme
参考文献
Zheng, Bin; Conlon, David A.; Corbett, R. Michael; Chau, Melissa; Hsieh, Dau-Ming; Yeboah, Agnes; Hsieh, Daniel; Mueslehiddinoglu, Jale; Gallagher, William P.; Simon, Jeffrey N.; Burt, Justin
Organic Process Research and Development, 2012 , vol. 16, # 11 p. 1846 - 1853