lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 24 h;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1209320', constants.ctx, '0')">sodium azide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '969209', constants.ctx, '0')">diethylene glycol</a> <br />T=135&deg;C;&nbsp;16&nbsp;h;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1209320', constants.ctx, '0')">sodium azide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '506008', constants.ctx, '0')">dimethyl sulfoxide</a> <br />T=90&deg;C;&nbsp;4&nbsp;h;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 90 percent / pyridine / 0 - 20 &deg;C<br />2: sodium azide / dimethylsulfoxide / 4 h / 90 &deg;C<br /> <br /> &nbsp;