1-氯-2,4,5-三甲基-苯合成路线 (共 10 条)
反应条件
2: H2SO4 3: quinoline / CuO View Scheme
参考文献
Newman,M.S. et al.
Journal of the American Chemical Society, 1962 , vol. 84, p. 995 - 997
反应条件
BnNMe3(1+)ICl4(1-) in acetic acid 20 h; Ambient temperature;
参考文献
Kajigaeshi, Shoji; Ueda, Yasuhiro; Fujisaki, Shizuo; Kakinami, Takaaki
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 6 p. 2096 - 2098
反应条件
chloroform; chlorine T=0°C;
参考文献
Smith; Moyle
Journal of the American Chemical Society, 1936 , vol. 58, p. 1,9
反应条件
chlorine; iodine in 1,1,2-trichloroethylene T=0°C; 0.0833333 h;
参考文献
Borodovitsyn, V. V.; Pozdnyakovich, Yu. V.; Shein, S. M.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 9 p. 1741 - 1746
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 9 p. 1937 - 1943
反应条件
chlorine; iodine in 1,1,2-trichloroethylene T=0°C; 0.0833333 h;
参考文献
Borodovitsyn, V. V.; Pozdnyakovich, Yu. V.; Shein, S. M.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 9 p. 1741 - 1746
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 9 p. 1937 - 1943
反应条件
sulfuryl dichloride; silica gel in tetrachloromethane T=25°C; 12 h;
参考文献
Borodovitsyn, V. V.; Pozdnyakovich, Yu. V.; Shein, S. M.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 9 p. 1741 - 1746
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 9 p. 1937 - 1943
反应条件
quinoline; copper(II) oxide
参考文献
Moffett; Tang
Journal of medicinal chemistry, 1968 , vol. 11, # 5 p. 1020 - 1022
反应条件
chlorine dioxide in water T=20°C; 24 h; Further byproducts.;
参考文献
Khasanova; Vozhdaeva; Kabal'nova; Kantor
Russian Journal of Applied Chemistry, 2007 , vol. 80, # 7 p. 1105 - 1110
参考文献
Smith; Moyle
Journal of the American Chemical Society, 1936 , vol. 58, p. 1,9
参考文献
Haller
Chemische Berichte, 1885 , vol. 18, p. 93