Wilkinson's catalyst in 1,4-dioxane T=135°C; 0.25 h; Inert atmosphere;

Wilkinson's catalyst in 1,4-dioxane T=135°C; 0.0125 h;

<b>Multi-step reaction with 2 steps<br /> </b>1.1: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / ethylene glycol dimethyl ether; water / 5 h / 80 &deg;C / |Inert atmosphere; |Schlenk technique<br />2.1: n-butyllithium / hexane; tetrahydrofuran / 0.42 h / -78 &deg;C / |Inert atmosphere; |Schlenk technique<br />2.2: 3.17 h / -78 - 20 &deg;C / |Inert atmosphere; |Schlenk technique<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1.1: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / ethylene glycol dimethyl ether; water / 5 h / 80 &deg;C / |Inert atmosphere; |Schlenk technique<br />2.1: n-butyllithium / hexane; tetrahydrofuran / 0.42 h / -78 &deg;C / |Inert atmosphere; |Schlenk technique<br />2.2: 3.17 h / -78 - 20 &deg;C / |Inert atmosphere; |Schlenk technique<br /> <br /> &nbsp;