1-甲基-4-丙-2-烯基磺酰基苯合成路线 （共 91 条）
参考文献
Backer; Strating; Drenth
Recueil des Travaux Chimiques des Pays-Bas, 1951 , vol. 70, p. 365,368, 371
反应条件
1-hydroxy-2(1H)-pyridinethione; 4-(N,N-dimethlyamino)pyridine in toluene T=110°C; 2 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1613 - 1620
反应条件
sodium hydride in tetrahydrofuran; mineral oil 3 h; Reflux;
参考文献
Tetrahedron, , vol. 69, # 46 p. 9616 - 9624
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate; tetrabutylammomium bromide; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene 16 h; Reflux;
参考文献
Le Duc, Gaetan; Bernoud, Elise; Prestat, Guillaume; Cacchi, Sandro; Fabrizi, Giancarlo; Iazzetti, Antonia; Madec, David; Poli, Giovanni
Synlett, 2011 , # 20 art. no. B17111ST, p. 2943 - 2946
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate; tetrabutylammomium bromide; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene 16 h; Reflux;
参考文献
Le Duc, Gaetan; Bernoud, Elise; Prestat, Guillaume; Cacchi, Sandro; Fabrizi, Giancarlo; Iazzetti, Antonia; Madec, David; Poli, Giovanni
Synlett, 2011 , # 20 art. no. B17111ST, p. 2943 - 2946
反应条件
nickel; acetic acid in n-heptane
参考文献
Boivin, Jean; Schiano, Anne-Marie; Zard, Samir Z.; Zhang, Haiwen
Tetrahedron Letters, 1999 , vol. 40, # 24 p. 4531 - 4534
反应条件
in various solvent(s)
T=180°C;
参考文献
Kumar, Perumal Raja
Journal of the Chemical Society, Chemical Communications, 1989 , p. 509 - 510
参考文献
Ueno, Yoshio; Aoki, Seiichi; Okawara, Makoto
Journal of the Chemical Society, Chemical Communications, 1980 , # 15 p. 683 - 684
反应条件
1.) THF-ether, -70 deg C, 30 min; 2.) -70 deg C, 135 min; Yield given. Multistep reaction;
参考文献
Knight, Derek J.; Lin, Peter; Russell, Simon T.; Whitham, Gordon H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2701 - 2706
反应条件
n-butyllithium in tetrahydrofuran; hexane
1) -78 deg C, 2) -30 deg C, 30 min;
参考文献
Julia, Marc; Righini-Tapie, Anne; Verpeaux, Jean-Noel
Tetrahedron, 1983 , vol. 39, # 20 p. 3283 - 3288
