5-乙酰氨基-2,4,6-三碘间苯二甲酰氯合成路线 (共 6 条)
反应条件
thionyl chloride in acetic acid
参考文献
Dibra S.p.A.
Patent: US5965772 A1, 1999 ;
参考文献
Guerbet S.A.
Patent: US4107286 A1, 1978 ;
反应条件
sulfuric acid in acetonitrile Product distribution / selectivity;
参考文献
MANAC INC.
Patent: WO2006/100731 A1, 2006 ;
Location in patent: Page/Page column 6 ;
反应条件
triethylamine in isobutyramide T=0 - 20°C; 13 h;
参考文献
IMPERIAL INNOVATIONS LIMITED; KINGS COLLEGE LONDON; GUYS AND ST THOMAS NHS FOUNDATION TRUST
Patent: WO2007/26140 A2, 2007 ;
Location in patent: Page/Page column 23; 25 ;
反应条件
hydrogenchloride in methanol; water; dimethylammonium 2,4-dichlorophenoxyacetate
参考文献
Dibra S.p.A.
Patent: US5965772 A1, 1999 ;
反应条件
in dimethylammonium 2,4-dichlorophenoxyacetate
参考文献
BRACCO S.p.A.; DIBRA S.p.A.
Patent: EP915835 B1, 2000 ;