6-(叠氮基甲基)-2,3-二氢苯并[b][1,4]二噁英盐酸盐合成路线 （共 3 条）
反应条件
hydrogenchloride in isopropyl alcohol T=25 - 30°C; pH=0.25 - 0.75;
参考文献
Natco Pharma Limited
Patent: US2010/298351 A1, 2010 ;
Location in patent: Page/Page column 34 ;
US 20100298351 A1
反应条件
hydrogenchloride; 5 palladium on charcoal; hydrogen in ethanol T=20°C; P=760.051 Torr;
参考文献
Su, Bo; Deng, Meng; Wang, Qingmin
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 5 p. 977 - 981
反应条件
1: hydroxylamine hydrochloride; sodium acetate / ethanol / 6 h / 20 °C 2: hydrogenchloride; hydrogen; 5 palladium on charcoal / ethanol / 20 °C / 760.05 Torr View Scheme
参考文献
Su, Bo; Deng, Meng; Wang, Qingmin
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 5 p. 977 - 981
