5-(4-甲基苯基)-1,3,4-噁二唑-2-硫醇合成路线 (共 10 条)
反应条件
1: With potassium hydroxide in ethanol T=0°C; 12 h; Reflux; 2: With hydrogenchloride in water pH=Ca. 5;
参考文献
Jha, Keshari Kishore; Samad, Abdul; Kumar, Yatendra; Shaharyar, Mohd.; Khosa, Ratan Lal; Jain, Jainendra; Kumar, Vikash; Singh, Priyanka
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 11 p. 4963 - 4967
反应条件
in dimethyl sulfoxide 0.00833333 h; Irradiation;
参考文献
Joshi, Sachin; Karnik
Synthetic Communications, 2002 , vol. 32, # 1 p. 111 - 114
反应条件
1: sulfuric acid 2: hydrazine hydrate / methanol 3: potassium hydroxide / ethanol View Scheme
参考文献
Journal of Agricultural and Food Chemistry, , vol. 60, # 4 p. 1036 - 1041
反应条件
1: hydrazine hydrate / methanol 2: potassium hydroxide / ethanol View Scheme
参考文献
Journal of Agricultural and Food Chemistry, , vol. 60, # 4 p. 1036 - 1041
反应条件
1: KOH 2: Heating View Scheme
参考文献
Heterocycles, , vol. 20, # 11 p. 2211 - 2224
反应条件
in N,N-dimethyl-formamide 0.05 h; Microwave irradiation; TemperatureTime;
参考文献
Mahesh Kumar; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2012 , vol. 51, # 11 p. 1619 - 1622
反应条件
1: hydrazine hydrate / ethanol / |Reflux 2: potassium hydroxide / ethanol / |Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 21, # 8 p. 2286 - 2297
反应条件
1: triethylamine / dichloromethane / 0 °C 2: hydrazine hydrate / methanol / 5 h / |Reflux 3: potassium hydroxide / methanol / 20 °C / |Reflux 4: hydrogenchloride / water / 0 - 5 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 1 p. 192 - 194
反应条件
Ambient temperature;
参考文献
Froeyen, Paul
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 57, # 1/2 p. 11 - 15
反应条件
Microwave irradiation;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 51, # 11 p. 1619 - 1622