1: benzyl alcohol With sodium hydride in tetrahydrofuran T=0°C; 1 h; 2: carbon dioxide in tetrahydrofuran T=0°C; 0.5 h; 3: benzyl chloroformate in tetrahydrofuran T=20°C; 18 h; Title compound not separated from byproducts;
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Johnston, Meghan; Bhatt, Shachi R.; Sikka, Surina; Mercier, Richard W.; West, Jay M.; Makriyannis, Alexandros; Gatley, S. John; Duclos Jr., Richard I.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 14 p. 4585 - 4592