2,4,6-三(4-氯苯基)-1,3,5-三嗪合成路线 (共 8 条)
反应条件
ammonia; lanthanum trifluoromethanesulphonate T=200°C; 24 h; in a stainless steel pressure vessel;
参考文献
Forsberg, John H.; Spaziano, Vincent T.; Klump, Stephen P.; Sanders, Kathleen M.
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 767 - 770
反应条件
trifluorormethanesulfonic acid in nitromethane T=100°C; 2 h; Yield given;
参考文献
El-Khagawa, Ahmed M.
Bulletin de la Societe Chimique de France, 1987 , # 2 p. 372 - 374
反应条件
ammonium hydroxide; Fremy’s salt in pyridine 168 h; Ambient temperature;
参考文献
Llobera, A.; Saa, J. M.; Peralta, A.
Synthesis, 1985 , # 1 p. 95 - 98
反应条件
[(Me3Si)2N]3Yb(μ-Cl)Li(THF)3 T=100°C; 24 h;
参考文献
Wang, Junfeng; Xu, Fan; Cai, Tao; Shen, Qi
Organic Letters, 2008 , vol. 10, # 3 p. 445 - 448
反应条件
ammonium hydroxide; Fremy’s salt in pyridine 168 h; Ambient temperature;
参考文献
Llobera, A.; Saa, J. M.; Peralta, A.
Synthesis, 1985 , # 1 p. 95 - 98
参考文献
Davis
Journal of the Chemical Society, 1905 , vol. 87, p. 1834
反应条件
sulfuric acid T=25°C;
参考文献
Bodrikov, I. V.; Michurin, A. N.; Vasyanina, G. I.; Bochkareva, N. N.; Krasnoj, V. L.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 12 p. 2123 - 2133
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 12 p. 2492 - 2503
反应条件
hydrogenchloride; aluminium trichloride
参考文献
DEGUSSA
Patent: DE959096 , 1952 ;
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DEGUSSA
Patent: US2769004 , 1953 ;