3-异丙基-2-甲基-1H-吲哚合成路线 （共 10 条）
反应条件
1-propanephosphonic acid cyclic anhydride in ethyl acetate T=100 - 150°C; Fischer indole synthesis; 0.25 h; Microwave irradiationSealed vessel;
参考文献
Desroses, Matthieu; Wieckowski, Krzysztof; Stevens, Marc; Odell, Luke R.
Tetrahedron Letters, 2011 , vol. 52, # 34 p. 4417 - 4420
反应条件
L-(+)-tartaric acid-urea melt T=70°C; Fischer Indole Synthesis; 1.5 h;
参考文献
Gore, Sangram; Baskaran, Sundarababu; Koenig, Burkhard
Organic Letters, 2012 , vol. 14, # 17 p. 4568 - 4571
反应条件
palladium diacetate; tetrabutyl-ammonium chloride; potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=100°C; 24 h;
参考文献
Larock; Yum; Refvik
Journal of Organic Chemistry, 1998 , vol. 63, # 22 p. 7652 - 7662
反应条件
triethylsilane; trifluoroacetic acid in dichloromethane T=0°C;
参考文献
Appleton, Julie E.; Dack, Kevin N.; Green, Andrew D.; Steele, John
Tetrahedron Letters, 1993 , vol. 34, # 9 p. 1529 - 1532
反应条件
methanesulfonic acid; phosphorus pentoxide 1) 3 d, 45 deg C 2) 1 d, 55 deg C 3) 1 d, 60 deg C; Yields of byproduct given;
参考文献
Zhao; Hughes; Bender; DeMarco; Reider
Journal of Organic Chemistry, 1991 , vol. 56, # 9 p. 3001 - 3006
反应条件
1: 1) 4-Angstroem sieves 2) acetic acid / toluene / 1) 6 h, 0 deg C 2) 15 h, 21 deg C 2: P2O5, MeSO3H / 1) 3 d, 45 deg C 2) 1 d, 55 deg C 3) 1 d, 60 deg C View Scheme
参考文献
Zhao; Hughes; Bender; DeMarco; Reider
Journal of Organic Chemistry, 1991 , vol. 56, # 9 p. 3001 - 3006
反应条件
1: 1) 4-Angstroem sieves 2) acetic acid / toluene / 1) 6 h, 0 deg C 2) 15 h, 21 deg C 2: P2O5, MeSO3H / 1) 3 d, 45 deg C 2) 1 d, 55 deg C 3) 1 d, 60 deg C View Scheme
参考文献
Zhao; Hughes; Bender; DeMarco; Reider
Journal of Organic Chemistry, 1991 , vol. 56, # 9 p. 3001 - 3006
反应条件
bis(1,5-cyclooctadiene)nickel (0); lithium tert-butylate; IPr*hydrochloride in toluene T=100°C; 12 h; Inert atmosphere;
参考文献
Yoshida, Yuji; Kurahashi, Takuya; Matsubara, Seijiro
Chemistry Letters, 2011 , vol. 40, # 10 p. 1067 - 1068
反应条件
1: 90 percent / NaH / tetrahydrofuran / 5 h / Heating 2: 13 percent / Bu3SnH; AIBN / toluene / 4 h / Heating View Scheme
参考文献
Palmieri, Alessandro; Petrini, Marino; Torregiani, Elisabetta
Tetrahedron Letters, 2007 , vol. 48, # 32 p. 5653 - 5656
参考文献
Itahara, Toshio; Ouya, Hiroshi; Kozono, Kiyotake
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 12 p. 3861 - 3864
