2,5-二甲氧基-1,4-苯醌合成路线 (共 69 条)
反应条件
in camphor-10-sulfonic acid
反应条件
sodium methylate in chloroform T=60°C; 2 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 33, # 7 p. 2983 - 2989
反应条件
(-)-10-CSA in toluene T=70°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 53, # 28 p. 9789 - 9798
反应条件
1: acetone; K2CO3 2: peroxybenzoic acid; CHCl3 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 74, p. 1305,1306
反应条件
1: ether BF3 2: diisopropylamine View Scheme
参考文献
Journal of the American Chemical Society, , vol. 78, p. 1233
参考文献
Journal of the American Chemical Society, , vol. 78, p. 1233
反应条件
dihydrogen peroxide; toluene-4-sulfonic acid; acetic acid T=80°C; Baeyer-Villiger oxidation; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 18 p. 7290 - 7296
反应条件
1: 5 percent aq. NaHCO3, pyridine / 0.03 h / 80 °C 2: diethyl ether / 0.5 h 3: 5 percent aq. NaHCO3 / ethanol / 80 °C 4: diethyl ether / 0.5 h View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 46, # 8 p. 1325 - 1329
反应条件
1: 5 percent aq. NaHCO3 / ethanol / 80 °C 2: diethyl ether / 0.5 h View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 46, # 8 p. 1325 - 1329
反应条件
1: diethyl ether / 0.5 h 2: 5 percent aq. NaHCO3 / ethanol / 80 °C 3: diethyl ether / 0.5 h View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 46, # 8 p. 1325 - 1329