5,6-二氢环戊烷并[b]吡啶-7-酮合成路线 （共 5 条）
反应条件
1: With oxygen; ozone in methanol; dichloromethane P=362.013 Torr; 1.5 amperes; 2: With thiourea in methanol; dichloromethane
参考文献
Allergan, Inc.
Patent: US2008/255239 A1, 2008 ;
Location in patent: Page/Page column 32 ;
US 20080255239 A1
反应条件
Dess-Martin periodane in dichloromethane
参考文献
Andreotti, Daniele; Miserazzi, Emanuele; Nalin, Arnaldo; Pozzan, Alfonso; Profeta, Roberto; Spada, Simone
Tetrahedron Letters, 2010 , vol. 51, # 50 p. 6526 - 6530
反应条件
1: 78 percent / Ac2O / 17 h / 170 °C / Heating 2: 1) ozone, 2) methyl sulfide / 1) CH3OH, -35 deg C, 2) -35 deg C, 0.5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 12 p. 2208 - 2212
反应条件
1: 2 h / 100 °C 2: potassium hydroxide / ethanol / 1 h / 20 °C 3: triethylamine; oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 24 h / -78 °C / |Inert atmosphere View Scheme
参考文献
Synlett, , vol. 24, # 7 art. no. ST-2012-D1091-L, p. 837 - 838
反应条件
1: potassium hydroxide / ethanol / 1 h / 20 °C 2: triethylamine; oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 24 h / -78 °C / |Inert atmosphere View Scheme
参考文献
Synlett, , vol. 24, # 7 art. no. ST-2012-D1091-L, p. 837 - 838
