4-氯-2,6-吡啶二甲醛合成路线 （共 3 条）
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 0.666667 h; 2: With hydrogenchloride in tetrahydrofuran; water
参考文献
Ivchenko, Pavel V.; Nifant'Ev, Ilya E.; Buslov, Ivan V.
Tetrahedron Letters, 2013 , vol. 54, # 3 p. 217 - 219
反应条件
1: With trifluoroacetic anhydride in dichloromethane; dimethyl sulfoxide T=-60 - 0°C; 4 h; 2: With triethylamine in dichloromethane; dimethyl sulfoxide T=20°C; 2.5 h; 3: With hydrogenchloride in dichloromethane; water; dimethyl sulfoxide
参考文献
Sensors for Medicine and Science
Patent: US2007/14726 A1, 2007 ;
Location in patent: Page/Page column 14 ;
反应条件
1: dichloromethane / 2 h / 0 - 20 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 0.67 h / 0 °C View Scheme
参考文献
Ivchenko, Pavel V.; Nifant'Ev, Ilya E.; Buslov, Ivan V.
Tetrahedron Letters, 2013 , vol. 54, # 3 p. 217 - 219
