5,10,15,20-四(4-吡啶基)-21H,23H-卟吩锌合成路线 (共 5 条)
反应条件
in methanol; chloroform 16 h; Inert atmosphere;
参考文献
Natali, Mirco; Luisa, Alessandra; Iengo, Elisabetta; Scandola, Franco
Chemical Communications, 2014 , vol. 50, # 15 p. 1842 - 1844
反应条件
in acetic acid refluxing porphyrin with slight excess of Zn-salt for 3 h; solvent removal, filtration, washing (H2O, CHCl3), drying (vac., overnight);
参考文献
Inorganica Chimica Acta, , vol. 267, # 2 p. 257 - 263
反应条件
1: pyridine-4-carbaldehyde; pyrrole With pyridine in methanol 24 h; Reflux; 2: Zn(CH3COO)2*2H2O
参考文献
Dalton Transactions, , vol. 43, # 2 p. 626 - 631
反应条件
in further solvent(s) TPyP extd. from CHCl3 into soln. of zinc complex in mixt. of perfluorohexanes (FC-72) to produce ZnTPyP complex; not isolated, detn. by UV-Vis spectroscopy;
参考文献
Journal of Physical Chemistry B, , vol. 113, # 21 p. 7449 - 7456
反应条件
in methanol; chloroform reflux, 20 h; chromy. (SiO2, CHCl3/EtOH/Py);
参考文献
Journal of Physical Chemistry B, , vol. 104, # 2 p. 271 - 278