异丙基氧代(苯基)乙酸酯合成路线 （共 33 条）
反应条件
in toluene T=0 - 20°C; Inert atmosphere;
参考文献
Infante, Rebeca; Nieto, Javier; Andres, Celia
Chemistry - A European Journal, 2012 , vol. 18, # 14 p. 4375 - 4379
反应条件
potassium isopropoxide in isopropyl alcohol T=75°C; 0.166667 h; Further byproducts given;
参考文献
Prato, Maurizio; Quintily, Ugo; Scorrano, Gianfranco
Gazzetta Chimica Italiana, 1984 , vol. 114, # 9/10 p. 405 - 412
反应条件
carbon monoxide; triethylamine in dimethyl sulfoxide 35 atm CO, presence of Et3N, N2-atmosphere, stirring for 30 min at 60°C; GC-anal., product selectivity detd.;
参考文献
Yamashita; Sakakura; Kobayashi; Tanaka
Journal of molecular catalysis, 1988 , vol. 48, # 1 p. 69 - 79
反应条件
oxygen in chloroform T=20°C; 30 h; Resolution of racemate; enantioselective reaction;
参考文献
Salunke, Santosh B.; Babu, N.Seshu; Chen, Chien-Tien
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 8 p. 1234 - 1240
反应条件
1: sodium hydroxide; water / 2 h / 20 °C 2: pyridine / dichloromethane / 1 h / 0 °C View Scheme
参考文献
Enders, Dieter; Stoeckel, Bianca A.; Rembiak, Andreas
Chemical Communications, 2014 , vol. 50, # 34 p. 4489 - 4491
反应条件
potassium isopropoxide in isopropyl alcohol T=75°C; 0.166667 h; Further byproducts given;
参考文献
Prato, Maurizio; Quintily, Ugo; Scorrano, Gianfranco
Gazzetta Chimica Italiana, 1984 , vol. 114, # 9/10 p. 405 - 412
反应条件
potassium isopropoxide in isopropyl alcohol T=75°C; 0.166667 h; Further byproducts given;
参考文献
Prato, Maurizio; Quintily, Ugo; Scorrano, Gianfranco
Gazzetta Chimica Italiana, 1984 , vol. 114, # 9/10 p. 405 - 412
反应条件
1: α,α-dibromo-1-phenylethanone With dimethyl sulfoxide T=70 - 75°C; Inert atmosphere; 2: isopropyl alcohol T=25 - 30°C; Inert atmosphere;
参考文献
Raghunadh, Akula; Meruva, Suresh Babu; Kumar, Nuka Anil; Kumar, Gudla Santosh; Rao, L. Vaikunta; Syamkumar
Synthesis, 2012 , vol. 2012, # 2 p. 283 - 289
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine T=60°C; P=114000 Torr; 24 h;
参考文献
Sakakura, Toshiyasu; Yamashita, Hiroshi; Kobayashi, Toshi-aki; Hayashi, Teruyuki; Tanaka, Masato
Journal of Organic Chemistry, 1987 , vol. 52, # 26 p. 5733 - 5740
反应条件
1: phosphorus tribromide / tetrahydrofuran 2: 4-methoxy pyridine; Ru(bpy)3Cl2; lithium carbonate / N,N-dimethyl acetamide / 24 h / 25 °C / Irradiation View Scheme
参考文献
Su, Yijin; Zhang, Liangren; Jiao, Ning
Organic Letters, 2011 , vol. 13, # 9 p. 2168 - 2171
