异丙基氧代(苯基)乙酸酯合成路线 （共 33 条）
反应条件
oxygen T=10°C; 2 h; Irradiation;
参考文献
Izawa; Ishiguro; Tomioka
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 5 p. 1490 - 1496
反应条件
carbon monoxide in isopropyl alcohol 30 atm CO, presence of Et3N, N2-atmosphere, mixing at -20°C, stirring for 1 h at 70°C; GC-anal., product selectivity detd.;
参考文献
Yamashita; Sakakura; Kobayashi; Tanaka
Journal of molecular catalysis, 1988 , vol. 48, # 1 p. 69 - 79
反应条件
carbon monoxide; triethylamine in not given 35 atm CO, presence of Et3N, N2-atmosphere, stirring for 30 min at 60°C; GC-anal., product selectivity detd.;
参考文献
Yamashita; Sakakura; Kobayashi; Tanaka
Journal of molecular catalysis, 1988 , vol. 48, # 1 p. 69 - 79
反应条件
in isopropyl alcohol T=75°C; 0.166667 h; Further byproducts given;
参考文献
Prato, Maurizio; Quintily, Ugo; Scorrano, Gianfranco
Gazzetta Chimica Italiana, 1984 , vol. 114, # 9/10 p. 405 - 412
反应条件
1.1: bromine / 1,4-dioxane / 25 - 30 °C / Inert atmosphere 2.1: dimethyl sulfoxide / 70 - 75 °C / Inert atmosphere 2.2: 25 - 30 °C / Inert atmosphere View Scheme
参考文献
Raghunadh, Akula; Meruva, Suresh Babu; Kumar, Nuka Anil; Kumar, Gudla Santosh; Rao, L. Vaikunta; Syamkumar
Synthesis, 2012 , vol. 2012, # 2 p. 283 - 289
反应条件
1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 20 °C / |Inert atmosphere 2: triethylamine / dichloromethane / 20 °C / |Inert atmosphere View Scheme
参考文献
Enders, Dieter; Stoeckel, Bianca A.; Rembiak, Andreas
Chemical Communications, 2014 , vol. 50, # 34 p. 4489 - 4491
反应条件
cobalt(II)salen; oxygen in 1,2-dichloro-ethane T=60°C; P=760 Torr; 8 h; var. cobalt Schiff's base complexes and Lewis acids as catalysts, var. reaction times; Rate constantProduct distribution;
参考文献
Maruyama, K.; Murakami, Y.; Yoda, K.; Mashino, T.; Nishinaga, A.
Journal of the Chemical Society, Chemical Communications, 1992 , # 21 p. 1617 - 1618
反应条件
carbon monoxide; triethylamine in N,N-dimethyl-formamide 40 atm CO, presence of Et3N, N2-atmosphere, stirring for 30 min at 60°C; GC-anal., product selectivity detd.;
参考文献
Yamashita; Sakakura; Kobayashi; Tanaka
Journal of molecular catalysis, 1988 , vol. 48, # 1 p. 69 - 79
反应条件
1: sulfuric acid / 3 h / Reflux 2: oxygen / chloroform / 30 h / 20 °C / Resolution of racemate View Scheme
参考文献
Salunke, Santosh B.; Babu, N.Seshu; Chen, Chien-Tien
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 8 p. 1234 - 1240
反应条件
in isopropyl alcohol T=75°C; 0.166667 h; Product distribution;
参考文献
Prato, Maurizio; Quintily, Ugo; Scorrano, Gianfranco
Gazzetta Chimica Italiana, 1984 , vol. 114, # 9/10 p. 405 - 412
