2,2,3,3-四(苯基)丁烷二腈合成路线 （共 37 条）
反应条件
1: PCl5; POCl3 2: sodium ethylate View Scheme
参考文献
Neure
Justus Liebigs Annalen der Chemie, 1889 , vol. 250, p. 143,147
反应条件
1: diethyl ether; NH3 / 230 °C / im geschlossenen Rohr 2: PCl5; POCl3 3: sodium ethylate View Scheme
参考文献
Neure
Justus Liebigs Annalen der Chemie, 1889 , vol. 250, p. 143,147
反应条件
1: glacial acetic acid; concentrated nitric acid 2: hydrochloride of tin dichloride; alcohol View Scheme
参考文献
Anschuetz; Romig
Justus Liebigs Annalen der Chemie, 1886 , vol. 233, p. 340
反应条件
1: glacial acetic acid; fuming nitric acid 2: hydrochloride of tin dichloride; alcohol View Scheme
参考文献
Anschuetz; Romig
Justus Liebigs Annalen der Chemie, 1886 , vol. 233, p. 340
反应条件
1: glacial acetic acid; concentrated nitric acid 2: hydrochloride of tin dichloride; alcohol View Scheme
参考文献
Anschuetz; Romig
Justus Liebigs Annalen der Chemie, 1886 , vol. 233, p. 340
参考文献
Neure
Justus Liebigs Annalen der Chemie, 1889 , vol. 250, p. 143,147
反应条件
n-butyllithium; 2-bromo-2-methylpropiophenon 1.) THF, liquid N2, 2.) r.t., 15 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Werry, Juergen; Stamm, Helmut; Sommer, Andreas
Chemische Berichte, 1990 , vol. 123, # 7 p. 1553 - 1562
反应条件
diethyl ether anschliessendes Behandeln mit Eis und wss. HCl;
参考文献
Smith
Chemische Berichte, 1938 , vol. 71, p. 634,641
参考文献
Aspelund
Chemische Berichte, 1930 , vol. 63, p. 1191,1193, 1196
Acta Academiae Aboensis, Series B: Mathematica et Physica, 1932 , vol. 6, # 17 p. 10
反应条件
samarium diiodide in tetrahydrofuran 0.0333333 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Yacovan, Avihai; Hoz, Shmaryahu
Journal of Organic Chemistry, 1997 , vol. 62, # 3 p. 771 - 772
