4-氧代-1,2,3,4-四氢萘-1-羧酸合成路线 (共 7 条)
反应条件
aluminium trichloride in nitrobenzene 5 h; Ambient temperature;
参考文献
Joshi; Samant
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 1 p. 22 - 25
反应条件
1: 90 percent / Ac2O / 3 h / Heating 2: 65 percent / AlCl3 / nitrobenzene / 5 h / Ambient temperature View Scheme
参考文献
Joshi; Samant
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 1 p. 22 - 25
反应条件
1: NaOEt 2: KOH / ethanol; H2O / Heating 3: 90 percent / Ac2O / 3 h / Heating 4: 65 percent / AlCl3 / nitrobenzene / 5 h / Ambient temperature View Scheme
参考文献
Joshi; Samant
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 1 p. 22 - 25
反应条件
1: amalgamated zinc; aqueous HCl 2: nach Abtrennung des Cinchonin-Salzes der (R)-1.2.3.4-Tetrahydro-naphthoesaeure-(1) (s.o.) ueber das Chinin-Salz View Scheme
参考文献
Westman
Arkiv foer Kemi, 1958 , vol. 12, p. 161,165
反应条件
methanol; sulfuric acid T=0 - 20°C; 20.5 h;
参考文献
Pfizer Inc
Patent: US2005/20616 A1, 2005 ;
Location in patent: Page/Page column 17 ;
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Ansell; Hey
Journal of the Chemical Society, 1950 , p. 2874,2880
反应条件
1: amalgamated zinc; aqueous HCl 2: ueber das Cinchonin-Salz View Scheme
参考文献
Westman
Arkiv foer Kemi, 1958 , vol. 12, p. 161,165