4,4,5,5-四甲基-2-(2-甲基-1-萘)-1,3,2-二噁硼烷合成路线 （共 6 条）
反应条件
copper(l) iodide; iron (III) acetylacetonate; N,N,N',N,-tetramethylethylenediamine; sodium hydride in tetrahydrofuran; mineral oil T=-10°C; Inert atmosphere;
参考文献
Labre, Flavien; Gimbert, Yves; Bannwarth, Pierre; Olivero, Sandra; Dunach, Elisabet; Chavant, Pierre Y.
Organic Letters, 2014 , vol. 16, # 9 p. 2366 - 2369
反应条件
potassium tetrachloropalladate; potassium acetate T=70°C; Miyaura borylation; 3 h; Inert atmosphere;
参考文献
Bej, Ansuman; Srimani, Dipankar; Sarkar, Amitabha
Green Chemistry, 2012 , vol. 14, # 3 p. 661 - 667
反应条件
in toluene 4 h; Heating;
参考文献
Cammidge, Andrew N.; Crepy, Karen V. L.
Tetrahedron, 2004 , vol. 60, # 20 p. 4377 - 4386
反应条件
1.1: Mg; I2 / tetrahydrofuran / 2 h / Heating 1.2: 60 percent / trimethyl borate / tetrahydrofuran / -78 - 20 °C 2.1: 86 percent / toluene / 4 h / Heating View Scheme
参考文献
Cammidge, Andrew N.; Crepy, Karen V. L.
Tetrahedron, 2004 , vol. 60, # 20 p. 4377 - 4386
反应条件
triphenylphosphine; cesium fluoride; palladium dichloride in ethylene glycol dimethyl ether Suzuki coupling; 72 h; Heating;
参考文献
Cammidge, Andrew N.; Crepy, Karen V. L.
Tetrahedron, 2004 , vol. 60, # 20 p. 4377 - 4386
反应条件
triphenylphosphine; cesium fluoride; palladium dichloride in ethylene glycol dimethyl ether Suzuki coupling; 72 h; Heating;
参考文献
Cammidge, Andrew N.; Crepy, Karen V. L.
Tetrahedron, 2004 , vol. 60, # 20 p. 4377 - 4386
